gabriel frances romero

- Relative’s preparation of many different instruments for the quantitative water analyze - Column’s preparation for ion pre-concentration and clean up. - Calibration of these instruments and control of the lamps. - Control quality of water (ammonium, sulphates, nitrates, mercury and Cr)

2008 2 months VIÑAS DEL VERO. Barbastro (Huesca) - Grapevine’s diary weight control according to a determinate collection. - Diary pH control and total acidity grapevine’s samples - Nitrogen’s determination of samples with a potenciometric analysis - Analysis of antocianos and poliphenol of samples with an spectrophotometer (520nm and 280nm) - Check of SO2 on wine samples - H2CO3 determination of samples extracted from the barrels - Determination of probably degree of grapevine’s s

- Physicochemical analyze : • Karl Fischer for water’s determination on raw material, pilot plant samples and final products(drugs) • Infrared spectroscopy (IR) to confirm drugs structure • Conductivity determination: Pilot plant samples and end products • Particule´s size determination • Determination of metals and sulphuric ashes from final product • Determination of Cl: Plant pilot’s samples by potenciometric determination - Instrumental techniques : • Synthesis product’s identification with H

NOVARTIS, DMPK Department (Head Lab Dr.R.Aichholz). Basel - Generation of drug metabolites by an analytical electrochemical cell(Analytical cells ESA 5011 and 5030) - Syntheses of drug metabolites using syntheses electrochemical cell(Syntheses cell ESA 5125) - Optimization of most important cell’s parameters( pH, flow, %organic phase) for achieve the best syntheses yield. - Compound’s detection performance by mass spectroscopy( ESI/MS: LTQ XL linear ion trap mass spectrometer, Thermo Fisher)